12 MINUTE READ
In this post, I will put forward an optimised method for the production of homemade vanilla extract and will discuss the factors that influence its quality. These include the bean quality, bean particle size, ethanol concentration, and ageing of the extract.
Table of Contents
1. The Vanilla Plant
Vanilla is a tropical epiphytic orchid of the family Orchidaceae (Childers et al., 1959). About 110 vanilla species have been identified, but only two are of commercial importance today: Vanilla planifolia Andrews, also known as Vanilla fragrans (Salisbury), and Vanilla tahitensis JW Moore (Purseglove et al., 1981). In the United States, these are the only species permitted to be used in food products. The main growing areas of Vanilla planifolia include the ‘Bourbon’ Islands (the term used collectively for beans from Madagascar, Reunion, Comoro Islands, and the Seychelles), Indonesia, Mexico, Tonga, and India, while Tahiti, Papua New Guinea, and limited parts of Indonesia produce mainly Vanilla tahitensis.
The fruit of a fully mature vanilla orchid is called a vanilla ‘pod’ or ‘bean’. These beans are green, long, smooth, and slender (somewhat resembling a large green bean), possess no flavour, and are almost odourless. To develop the characteristic vanilla flavour and aroma, green beans are subjected to a curing process commonly lasting three to six months. When properly cured, vanilla beans should resemble long, very thin cigarillos; supple, very dark brown, a raisin-like texture and somewhat oily sheen. High-quality beans may have white crystals of vanillin clinging to the outside, but this is rarely seen today (Gillette & Hoffman, 2000).
Cured vanilla beans can be used as they are, but the vast majority are used for the extraction and the preparation of vanilla products, of which there are four basic types: vanilla extract, by far the most used vanilla product, vanilla oleoresin, vanilla absolute, and vanilla powder/sugar.
2. Vanilla Extract
2.1 Definition
In the U.S Code of Federal Regulations for Vanilla, 21CFR169.175 169.182, vanilla extract is defined as the solution in aqueous ethyl alcohol of the sapid and odorous principles extractible from vanilla beans. In vanilla extract, the content of ethyl alcohol is not less than 35 percent by volume and the content of vanilla constituent is not less than one unit per gallon.
The term ‘unit’ means, in the case of vanilla beans containing not more than 25 percent moisture, 13.35 ounces of such beans, and, in the case of vanilla beans containing more than 25 percent moisture, it means the weight of such beans equivalent in content of moisture-free vanilla bean solids to 13.35 ounces of vanilla beans containing 25 percent moisture. This amounts to not less than 10.0125 oz (FDA standard) of dry weight solids.
Vanilla extract may contain one or more of the following ingredients:
- Glycerin
- Propylene glycol (usually no more than 2%)
- Sugar (including invert sugar)
- Dextrose
- Corn Syrup (or corn syrup solids)
2.2 What is vanilla ‘fold’?
The concentration of an extract is noted by its ‘fold’, with vanilla extracts available in 1 to 10 fold strength. A single fold of vanilla extract contains the extractable material from 13.35 oz of vanilla beans per gallon of solvent, or 100g of extractable material per litre, whereas a ten-fold product contains the extractable material from 1kg of beans per 1 litre of solvent. Almost all household extracts are single-fold strength, with two-fold and higher strength extracts being preferred by industrial food manufacturers.
2.3 What influences the quality of vanilla extract?
Several factors influence the quality of vanilla extract. These include 1. the quality of the beans, 2. bean particle size, 3. ethanol concentration, and 4. appropriate period of ageing (Broderick, 1955; Merory, 1969; Heath and Reineccius, 1986).
2.3.1 Bean quality
Most experts generally consider the flavour of a high vanillin (>0.20%), high moisture (>20%) Bourbon bean to deliver the best quality extract.
2.3.1.1 A high vanillin content
Although vanilla extract contains more than 300 compounds (Toth et al., 2011), the most commonly associated with vanilla extract quality are 3-methoxy-4-hydroxybenzaldehyde (vanillin), vanillic acid, p-hydroxybenzaldehyde, and p-hydroxybenzoic acid (Havkin-Frenkel et al., 2011). Of these, vanillin is the most abundant and generally used as the prime indicator of flavour quality of extracts: the lower the vanillin content, the lower the flavour quality of the bean will be, not just because of the vanillin itself, but also due to the other flavour notes which develop along with vanillin during curing.
Vanillin is present in single-fold extracts at levels ranging from 0.2 per 100 ml (0.2%) for a good quality extract to less than 0.02 per 100 mL (0.02%) for inferior quality product (Ranadive, 2011). Vanilla extracts made from Indian vanilla beans tend to yield vanillin content in the range of 0.2 to 0.25% per fold, whereas beans from Madagascar are averaging less than 0.18% vanillin content per fold (Ranadive, 2011).
The vanillin content alone does not, however, constitute vanilla flavour; vanillin alone is probably responsible for no more than 25% of the character of quality vanilla extract. Gillette & Hoffman (2000) note that flavour notes such as pruney, woody, floral, fruity, and rummy, which develop along with vanillin during curing, are even more important than vanillin character alone. In some cases, extracts with high amounts of vanillin will not taste as good as other extracts with lower vanillin content but containing the other flavour components
2.3.1.2 Moisture Content
The moisture content of commercial vanilla beans varies from 10% for poor quality lower grade beans to 35% for gourmet beans (Ranadive, 2011). ‘Extraction’ grade beans contain from 20 to 25% moisture, the maximum limit set by the US standard of identity. Drier beans are less aromatic than high moisture beans and flavour notes, such as pruney, woody, floral, fruity, and rummy, which develop along with vanillin during curing, do not develop and/or are lost, in over-dried (low moisture) beans (Gillette & Hoffman, 2000).
2.3.2 Bean particles size
Dong et al. (2013) compared three different bean particle sizes (2mm and 5mm chopped beans, and powdered beans) in the production of vanilla extract using Microwave-Assisted Extraction (MAE). Their results showed that vanillin yield increased with decreasing particle sizes: powdered beans had higher yield than that of chopped vanilla beans. The researchers also found that sloshing around the container of the powdered vanilla beans improved the extraction efficiency of the beans.
The vanillin yields at different bean particle sizes. Dong et al. (2014)
2.3.3 Ethanol Concentration
The extraction of vanillin from cured vanilla beans is greatly influenced by the ethanol percentage in the solvent. Changes in ethanol concentration mainly affect the polarity (whether a liquid will mix with another liquid) of the solvent. Dong et al. (2013) found that a 70% ethanol concentration may possess similar polarity to vanillin and give a higher yield than 40% and 100% ethanol concentrations. Jadhav et al. (2009) found that when the ethanol volume percentage in the solvent was lower than 50% (v/v) during conventional extraction, the extraction increased with the increase of ethanol concentration (from about 85 ppm at 30% ethanol to about 120 ppm of vanillin extraction at 50% ethanol). However, beyond this concentration, any further increase was found to be detrimental for the extraction process (the extent of vanillin extraction decreased gradually to about 105 ppm for 100% ethanol). Thus, a 1:1 v/v ethanol/water solution resulted in maximum extraction of vanillin from cured vanilla beans during conventional extraction.
2.3.4 Ageing
Freshly made vanilla extract has a slightly harsh alcohol bite, unless tempered with the addition of sugar syrup or glycerin. Like a fine wine, the flavour of vanilla extract mellows and improves as it ages. A minimum of 60 days ageing of a finished extract is advisable to develop the resinous, Bourbon character fully (Gillette & Hoffman, 2000). Stored under proper conditions (60-65°F) and away from light, vanilla develops pleasant, sweet, somewhat complex and mellow notes (Ranadive, 2011). Vanilla extract continuous to improve over a several year period until it more resembles a delightful liquor than vanilla extract. Storage in oak barrels (new or previously used for whiskey) is a traditional method for vanilla.
2.4 How to make a single-fold vanilla extract
This process yields about 500ml of vanilla extract. Weigh 50g of grade A beans. In a spice, or coffee, grinder, finely grind the beans and add to a 500ml glass jar. Add 250ml of 50% vodka and close the jar. Leave to steep at room temperature for at least 12 hours, sloshing the ground beans around the jar once every hour. Decant the extract into a separate 500ml glass jar using a fine sieve to remove the ground beans. Close the jar and store at room temperature and away from light. Place the sieved ground beans back into the first jar and add 250ml of fresh 50% vodka. Close the jar and leave to infuse at room temperature for at least 12 hours, sloshing the ground beans around the jar once every hour. At the end of this period, decant the extract into the jar containing the first extract using a fine sieve to remove the ground beans, which can now be discarded. The combined solutions produce a complete and full-bodied extract. Bring the volume of the combined extract to 500ml with the addition of 50% vodka, if required. Shake well. Age the extract for a minimum of 60 days at 60°F to 65°F (16°C to 18°C) and away from light.
3. References
Broderick, J. J., 1955. Vanilla extract manufacture. A guide to choice of method. Food Manuf., 30(1): 65–8.
Childers, N. F., Cibes, H. R., and Hernande-Medina, E., Vanilla – the orchid of commerce. In: Wither, C. L. ed. 1959. The Orchids, a Scientific Survey. New York: Ronald Press. Pp 477-508.
Dong, Z., Gu, F., Xu, F., and Wang, Q., 2014. Comparison of four kinds of extraction techniques and kinetics of microwave-assisted extraction of vanillin from Vanilla planifolia Andrews. Food Chemistry. 149. 54-61.
Gillette, M., and Hoffman, P., 2000. Vanilla extract. In: Francis, F.J. ed. 2000. Encyclopedia of Food Science and Technology. 2nd Edn. John Wiley & Sons, New York, pp. 2383–2399.
Havkin-Frenkel, D., Belanger, F. C., Booth, D. Y. J., Galasso, K. E., Tangel, F. P., and Gayosso, C. J. H. A Comprehensive Study of Composition and Evaluation of Vanilla Extract in US Retail Stores. In: Havkin-Frenkel, D., and Belanger, F. C., ed. 2011. Handbook of Vanilla Science and Technology. Blackwell Publishing Ltd.
Heath, H. B., and Reineccius, G., 1986. Flavor Chemistry and Technology. AVI, CT. Westport.
Jadhav, D., Rekha, B. N., Gogate, P. R., Rathod, V. K., 2009. Extraction of vanillin from vanilla pods: A comparison study of conventional soxhlet and ultrasound assisted extraction. Journal of Food Engineering. 93. 421-426.
Merory, J., 1960. Food Flavorings: Composition, Manufacture and Use. AVI, Westport, CT.
Purseglove, J. W., Brown, E. G., Green, C. L., and Robbins, S. R. J., 1981. Spices, Vol 2, New York, Longman, Inc.
Ranadive, A. S. Quality Control of Vanilla Beans and Extracts. In: Havkin-Frenkel, D., and Belanger, F. C. ed. 2011. Handbook of Vanilla Science and Technology. Blackwell Publishing Ltd.
Rao, S. R., and Ravishankar, G. A., 2000. Review Vanilla flavour: production by conventional and biotechnological routes. Journal of the Science of Food and Agriculture. 80:289-304
Toth, S., Joong Lee, K., Havkin-Frenkel, D., Belanger, F. C., and Hartman, T., G. Volatile Compounds in Vanilla. In: Havkin-Frenkel, D., and Belanger, F. C. ed. 2011. Handbook of Vanilla Science and Technology. Blackwell Publishing Ltd.
Ruben-
Thank you for all the homework you did preparing this web page. One question: when you say “50% vodka” or “50% ethanol,” is that by weight (1 g of ethanol to 1 g of water) or by volume (1 liter of ethanol to 1 liter of water)?
Thanks.
Hi Ruben! I just found this article and it’s the best information I’ve seen anywhere about making vanilla extract. Here in California, I can get Everclear 120, which is 60% alcolhol. I’m planning to try your recipe with that, then age it in an oak barrel before bottling. Is there any benefit or detriment to leaving the beans in the alcohol longer?
Hey John! Thanks for getting in touch. I hope you find the information on vanilla extract useful. Ageing in an oak barrel is an excellent idea; I’ve been meaning to test this for a long time now to see what effect it has on flavour but just haven’t had the time. He longer you can leave the ground beans infusing the alcohol the better because more of the water-soluble flavour compounds will be extracted. I’d also recommending agitating the mix from time to time, possibly by shaking the barrel, to extract more flavour. Please do let me know how you get on with your extract in your oak barrel.
All the best,
Ruben
I am so grateful to you scientist-ice cream makers out there. I am using grade B beans. Originally I used a whole bean for each recipe using your standard formula, but the flavor was too intense. Now I use 1/2 bean, scraped out.
If forced to choose between using grade B beans vs extract from Grade A beans, which would you opt for?)
Try cutting back on the sugar of the vanilla flavour is too intense. I need to update my recipe. That’s a very good question, can you not use both? That’s a difficult one to answer without testing both but probably the grade B beans, that’s just my gut feeling though; can’t emphasise enough the importance of testing both!
Sigh. That’s the difference between real scientists and the rest of us. I’ll try and report back.
Hey Roger, any luck with the vanilla?
Not yet. I have been focused on my Halwa ice cream. Would love to talk to you about my recipe if you are interested.
Sure, always happy to talk ice cream! 🙂
I have always used vanilla beans in my ice cream. One half bean in one of your recipes. Do you think good quality vanilla extract produces a better flavor, or a bean cooked in the mix?
Hi Roger, apologies for the late reply; been a bit hectic here. No using just vanilla extract doesn’t come close to the intensity of vanilla from a bean, especially with commercial extracts. Extract compliments the flavour from the bean, especially in high fat mixes, by giving you a quick initial burst of vanilla flavour as the volatiles molecules in the alcohol evaporate. The bean gives the strong, delayed flavour a few seconds after you swallow the ice cream.
I have 4 batches of homemade vanilla extract using different amounts of bean and different alcohol contents that I want to test against ice cream made using a vanilla bean.
Hi Ruben!. I read your vanilla extract post and have a a few questions for you. 1.- why not directly infuse the 50 gr vanilla beans into the 500 ml vodka directly? I am sorry I do not understand why infusing the 50 grs vanilla into 250 ml first and then sieve and put the same beans into the rest (the other 250ml) of the vodka.
2.- My second question is in relation with the alcohol percentage. I am sorry but I am a little confused: the article mentions 30%, 70% alcohol, 40% alcohol and 50 % alcohol as the ideal ranges for alcohol in vanilla extract. Then the suggested recipe says to use 50% alcohol vodka. Is 50% alcohol content by volume better than the traditional 40% alcohol content vodka? I really did not understand that part :(.
3.- I bought 1 lb vanilla beans (B grade) and infused it in 40% vodka, but I did not grind the beans
(I opened the beans and scraped the seeds one by and then just put the empty pod inside the vodka container where the seeds and vodka is. The reason I did not chop the beans finely, is because I was planning to reuse it to make vanilla sugar., also, I thought that grinding the beans would cause the liquid to be very filled with plenty and particles and I would be having to thoroughly sieve it. And I wanted to have vanilla seeds / caviar from the beans in the extract, but if I infuse it I am afraid all of the seeds will get wasted because they will blend/mix with the grinded pod. and therefore when sieving the solids from all of the vodga (seeds included ) would get wasted.But please tel me, Is is really better to grind up the vanilla beans? I am not planning to give it away. I will just infuse in the bottles where it is infusing for at least 2 years and then, start using from the bottles without removing the beans or seeds from the bottle… so it will continue to infuse indefinitely… Please be so kind to let me know your thoughts on all this..
Thank you, Ruben.
Hi there Lilie!
Thanks for getting in touch and happy new year to you! That’s a good question. Infusing 50g of beans with 250ml of the vodka, decanting, and then infusing the same beans in another 250ml of vodka is supposed to produce a complete and full-bodied extract. I suspect that this has something to do with more flavour molecules being extracted by an alcohol solution that contains fewer vanilla solids (which means that fresh alcohol will extract more flavour molecules than alcohol that already contains a lot of flavour molecules), although I don’t fully understand this. I haven’t tested this myself but intend to see whether there is a difference in flavour between an extract made with one wash of 500ml of vodka and left for say 2 days, compared to one that is made with two separate washes of 250ml of alcohol and, combined, left the same amount of time. If you try this experiment yourself, I’d love to hear your results.
The ideal ethanol concentration of the vodka appears to be 70%; this will give a higher yield of vanillin than 30%, 40%, and 50% ethanol vodka. You’re right that the recipe for a standard one-fold extract is confusing as it calls for 50% ethanol vodka so I’ll be updating this shortly to change the 50% ethanol vodka to the optimum 70% ethanol vodka concentration. In answer to your question, yes 50% ethanol vodka is better than 40% ethanol vodka, but 70% ethanol vodka appears to be optimum.
I’d recommend using grade A beans if you can as these will give a much better flavour than grade B, but you will pay quite a bit more. Yes I’d highly recommend grinding your beans in a spice grinder or cutting them into as many small pieces as you can as this will increase the surface area of the beans, which will mean that more flavour is extracted. I’d also recommend shaking the jar that you’re using very now and again; the more shaking or agitating you can do, the more flavour will be extracted from the beans.
You could always infuse the sieved bean solids with sugar to make your vanilla sugar, although this may then make separating the vanilla solids and sugar a little more difficult. You may have to chose between a stronger vanilla extract with chopped or ground beans, or vanilla sugar with whole beanas!
Yes if you chop or grind the beans, you will then have to sieve your extract but this won’t remove all of the small seeds; a lot will get through the sieve and remain in your extract.
I hope that answers your questions. Let me know if you need help with anything else.
All the best,
Ruben
Happy New Year to you too, Ruben!
Thank you for your reply.
I already went ahead and made sure to grind all of the beans I had, and put them already in the 40% vodka I had. Unfortunately I had already previously bought three bottles of 1.75ml each, in order to make the extract. It was afterwards that I found your beautiful website. Since I dont like to drink alcohol, I had to use them for the extract because I would have otherwise wasted the liquid… Also, I wanted to tell you that I have not heard of 70% alcohol content beverages.. I was very surprised to read about the study in relation to the alcohol content and the purity of the vanilla extraction. I am a little worried about the extract being overwhelmingly potent (I mean the alcohol). Tell me, have you tried this already? Sounds so very interesting and if you have made vanilla extract with the regular 40% alcohol and then tried to make it with the 50% or the 70% I would love to know your thoughts about it 🙂
Thank you again, Ruben!
Hahaha, sorry Ruben!, I meant three bottles of 1.75 liters, each. 🙂
Hey again Lilie!
Yes you’re right in that I don’t think you can buy 70% alcohol beverages but you can dilute some ethanol with water to get a 70% ethanol mix. I’ve seen a 50% vodka for sale here in the UK. If you make another batch of vanilla extract, I’d recommend trying to get hold of 50% vodka if you can.
You can age the extract for a minimum of 2 months if you’re worried about your extract being overwhelmingly potent. The longer you age it, the more it will mellow. I haven’t yet tried using a 70% alcohol mix myself to make vanilla extract. I have a 3 year old extract that I made using 40% vodka and beans and intend to compare this to one made with 50% and 70% alcohol when I get the time. I’ll let you know when I do this.
All the best,
Ruben
Hello Ruben !
Have you ever heard about the “rapid infusion” method under pressure inside a cream whipper made popular by Dave Arnold ?
In generell it is interesting for the purpose to make an extract very fast – for instance with fresh leaves from herbs.
Eventually it is also an use full method for vanilla extract or coffee extract.
I myself have no experiences with this technology but thought it would perhaps have potential for you for some flavouring purposes.
Regards, Christian
Hi there Christian!
I haven’t heard of the rapid infusion technique so many thanks for bringing it to my attention. I wonder how strong a vanilla extract made using this technique would be because it doesn’t sound like the ethanol/water solution stay in contact with the beans for very long. Looks interesting though!
All the best,
Ruben